Crystallography Open Database

Information card for entry 4087592

Preview

Coordinates	4087592.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H18 Cr2 D12 O6 Pd2
Calculated formula	C36 H18 Cr2 D12 O6 Pd2
Title of publication	Stabilization of an Electron-Unsaturated Pd(I)‒Pd(I) Unit by Double Hemichelation
Authors of publication	Werlé, Christophe; Karmazin, Lydia; Bailly, Corinne; Ricard, Louis; Djukic, Jean-Pierre
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	12
Pages of publication	3055
a	8.286 ± 0.001 Å
b	11.934 ± 0.001 Å
c	16.148 ± 0.001 Å
α	90°
β	100.525 ± 0.001°
γ	90°
Cell volume	1569.9 ± 0.3 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0458
Residual factor for significantly intense reflections	0.0389
Weighted residual factors for significantly intense reflections	0.0813
Weighted residual factors for all reflections included in the refinement	0.0843
Goodness-of-fit parameter for all reflections included in the refinement	1.178
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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