Information card for entry 4087622

Structure parameters

• Formula: C25 H38 P2 Pd
• Calculated formula: C25 H38 P2 Pd
• Title of publication: C‒H Activation Reactions of a Nucleophilic Palladium Carbene
• Authors of publication: Comanescu, Cezar C.; Iluc, Vlad M.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 19
• Pages of publication: 4684
• a: 9.059 ± 0.0015 Å
• b: 23.63 ± 0.004 Å
• c: 11.5744 ± 0.0018 Å
• α: 90°
• β: 92.664 ± 0.003°
• γ: 90°
• Cell volume: 2475 ± 0.7 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0453
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for significantly intense reflections: 0.0795
• Weighted residual factors for all reflections included in the refinement: 0.0812
• Goodness-of-fit parameter for all reflections included in the refinement: 1.139
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No