Information card for entry 4087701

Structure parameters

• Formula: C112 H114 N Nb O2 P
• Calculated formula: C112 H114 N Nb O2 P
• Title of publication: Anionic and Mononuclear Phosphinidene and Imide Complexes of Niobium
• Authors of publication: Searles, Keith; Carroll, Patrick J.; Mindiola, Daniel J.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 19
• Pages of publication: 4641
• a: 14.617 ± 0.0008 Å
• b: 14.9975 ± 0.0008 Å
• c: 21.2515 ± 0.0012 Å
• α: 70.619 ± 0.003°
• β: 89.292 ± 0.004°
• γ: 85.567 ± 0.003°
• Cell volume: 4381.1 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1901
• Residual factor for significantly intense reflections: 0.0779
• Weighted residual factors for significantly intense reflections: 0.1607
• Weighted residual factors for all reflections included in the refinement: 0.2082
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No