Information card for entry 4087831

Structure parameters

• Formula: C24 H28 F18 Mo N2 O3
• Calculated formula: C24 H28 F18 Mo N2 O3
• Title of publication: Synthesis of Molybdenum and Tungsten Alkylidene Complexes that Contain atert-Butylimido Ligand
• Authors of publication: Jeong, Hyangsoo; Schrock, Richard R.; Müller, Peter
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 17
• Pages of publication: 4408
• a: 16.5372 ± 0.0008 Å
• b: 17.6547 ± 0.0009 Å
• c: 21.0898 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6157.4 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0314
• Residual factor for significantly intense reflections: 0.0249
• Weighted residual factors for significantly intense reflections: 0.0593
• Weighted residual factors for all reflections included in the refinement: 0.0627
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No