Information card for entry 4087949

Structure parameters

• Formula: C37 H81 Ge2 K O7 Si6
• Calculated formula: C37 H81 Ge2 K O7 Si6
• Title of publication: Stable Germenolates and Germenes with Exocyclic Structures
• Authors of publication: Haas, Michael; Leypold, Mario; Schnalzer, Dominik; Torvisco, Ana; Stueger, Harald
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 21
• Pages of publication: 5291
• a: 21.674 ± 0.0009 Å
• b: 10.6653 ± 0.0005 Å
• c: 22.5781 ± 0.0009 Å
• α: 90°
• β: 92.411 ± 0.002°
• γ: 90°
• Cell volume: 5214.5 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0616
• Residual factor for significantly intense reflections: 0.0389
• Weighted residual factors for significantly intense reflections: 0.0863
• Weighted residual factors for all reflections included in the refinement: 0.0955
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No