Information card for entry 4088173

Structure parameters

• Chemical name: Tetraethylammonium (?2-carbonyl)-(?2-hydrido)-(?3-hydridoarsinidene)-decacarbonyl-tri-iron
• Formula: C19 H22 As Fe3 N O11
• Calculated formula: C19 H22 As Fe3 N O11
• Title of publication: Transformations in Transition-Metal Carbonyls Containing Arsenic: Exploring the Chemistry of [Et4N]2[HAs{Fe(CO)4}3] in the Search for Single-Source Precursors for Advanced Metal Pnictide Materials
• Authors of publication: Schipper, Desmond E.; Young, Benjamin E.; Whitmire, Kenton H.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 4
• Pages of publication: 471
• a: 19.346 ± 0.003 Å
• b: 14.5605 ± 0.0018 Å
• c: 20.15 ± 0.003 Å
• α: 90°
• β: 105.846 ± 0.006°
• γ: 90°
• Cell volume: 5460.3 ± 1.4 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.049
• Residual factor for significantly intense reflections: 0.0349
• Weighted residual factors for significantly intense reflections: 0.0764
• Weighted residual factors for all reflections included in the refinement: 0.0872
• Goodness-of-fit parameter for all reflections included in the refinement: 1.13
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No