Information card for entry 4088227

Structure parameters

• Formula: C31 H51 N9 U
• Calculated formula: C31 H51 N9 U
• Title of publication: Synthetic Utility of Tetrabutylammonium Salts in Uranium Metallocene Chemistry
• Authors of publication: Webster, Christopher L.; Langeslay, Ryan R.; Ziller, Joseph W.; Evans, William J.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 4
• Pages of publication: 520
• a: 18.9445 ± 0.001 Å
• b: 16.9108 ± 0.0009 Å
• c: 19.7306 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6321 ± 0.6 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0259
• Residual factor for significantly intense reflections: 0.0187
• Weighted residual factors for significantly intense reflections: 0.0436
• Weighted residual factors for all reflections included in the refinement: 0.0464
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No