Information card for entry 4088230

Structure parameters

• Formula: C39.5 H70 Cl2 N2 O3 U
• Calculated formula: C39.5 H70 Cl2 N2 O3 U
• Title of publication: Synthetic Utility of Tetrabutylammonium Salts in Uranium Metallocene Chemistry
• Authors of publication: Webster, Christopher L.; Langeslay, Ryan R.; Ziller, Joseph W.; Evans, William J.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 4
• Pages of publication: 520
• a: 11.2214 ± 0.0005 Å
• b: 11.7908 ± 0.0005 Å
• c: 17.7903 ± 0.0008 Å
• α: 77.9253 ± 0.0005°
• β: 88.4904 ± 0.0005°
• γ: 65.5842 ± 0.0005°
• Cell volume: 2091.12 ± 0.16 ų
• Cell temperature: 88 ± 2 K
• Ambient diffraction temperature: 88 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0237
• Residual factor for significantly intense reflections: 0.0202
• Weighted residual factors for significantly intense reflections: 0.0474
• Weighted residual factors for all reflections included in the refinement: 0.0486
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No