Information card for entry 4088265

Structure parameters

• Formula: C16 H21 F6 O6 P Si2 W
• Calculated formula: C16 H21 F6 O6 P Si2 W
• Title of publication: C-Trifluoromethyl-Substituted 1,2-Oxaphosphetane Complexes: Synthetic and Structural Study
• Authors of publication: Kyri, Andreas W.; Schnakenburg, Gregor; Streubel, Rainer
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 4
• Pages of publication: 563
• a: 8.9748 ± 0.0009 Å
• b: 10.3623 ± 0.0009 Å
• c: 15.417 ± 0.0013 Å
• α: 70.869 ± 0.005°
• β: 79.168 ± 0.006°
• γ: 66.889 ± 0.005°
• Cell volume: 1243 ± 0.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0747
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.1034
• Weighted residual factors for all reflections included in the refinement: 0.117
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No