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Information card for entry 4088319
Preview
Coordinates | 4088319.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C81 H99 B2 Cl8 F8 N2 O2 P2 Pd |
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Calculated formula | C81 H92 B2 Cl8 F8 N2 O2 P2 Pd |
Title of publication | Pd(II) Complexes Ligated by 1,3-Bis(diphenylphosphino)calix[4]arene: Preparation, X-ray Structures, and Catalyses |
Authors of publication | Hirasawa, Kengo; Tanaka, Shinya; Horiuchi, Takeru; Kobayashi, Takahiro; Sato, Takumi; Morohashi, Naoya; Hattori, Tetsutaro |
Journal of publication | Organometallics |
Year of publication | 2016 |
Journal volume | 35 |
Journal issue | 3 |
Pages of publication | 420 |
a | 18.2799 ± 0.0017 Å |
b | 19.204 ± 0.0019 Å |
c | 24.661 ± 0.002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 8657.2 ± 1.4 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 9 |
Space group number | 62 |
Hermann-Mauguin space group symbol | P n m a |
Hall space group symbol | -P 2ac 2n |
Residual factor for all reflections | 0.1367 |
Residual factor for significantly intense reflections | 0.0975 |
Weighted residual factors for significantly intense reflections | 0.2353 |
Weighted residual factors for all reflections included in the refinement | 0.2626 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.173 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4088319.html
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