Crystallography Open Database

Information card for entry 4088535

Preview

Coordinates	4088535.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H53 Cl3 Li N6 O4 Sc
Calculated formula	C31.97 H52.92 Cl3 Li N6 O4 Sc
Title of publication	Tris(pyrazolyl)methanide Complexes of Trivalent Rare-Earth Metals
Authors of publication	Li, Tengfei; Zhang, Guangchao; Guo, Jingjing; Wang, Shaowu; Leng, Xuebing; Chen, Yaofeng
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	10
Pages of publication	1565
a	12.5688 ± 0.0012 Å
b	12.5688 ± 0.0012 Å
c	43.147 ± 0.005 Å
α	90°
β	90°
γ	120°
Cell volume	5902.9 ± 1.1 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	7
Space group number	161
Hermann-Mauguin space group symbol	R 3 c :H
Hall space group symbol	R 3 -2"c
Residual factor for all reflections	0.0759
Residual factor for significantly intense reflections	0.0612
Weighted residual factors for significantly intense reflections	0.1735
Weighted residual factors for all reflections included in the refinement	0.1886
Goodness-of-fit parameter for all reflections included in the refinement	1.061
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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