Information card for entry 4088537

Structure parameters

• Formula: C32 H53 Cl3 Li Lu N6 O4
• Calculated formula: C31.9996 H52.9992 Cl3 Li Lu N6 O4
• Title of publication: Tris(pyrazolyl)methanide Complexes of Trivalent Rare-Earth Metals
• Authors of publication: Li, Tengfei; Zhang, Guangchao; Guo, Jingjing; Wang, Shaowu; Leng, Xuebing; Chen, Yaofeng
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 10
• Pages of publication: 1565
• a: 12.5731 ± 0.0012 Å
• b: 12.5731 ± 0.0012 Å
• c: 43.468 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5950.9 ± 1 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 7
• Space group number: 161
• Hermann-Mauguin space group symbol: R 3 c :H
• Hall space group symbol: R 3 -2"c
• Residual factor for all reflections: 0.0464
• Residual factor for significantly intense reflections: 0.028
• Weighted residual factors for significantly intense reflections: 0.0721
• Weighted residual factors for all reflections included in the refinement: 0.0814
• Goodness-of-fit parameter for all reflections included in the refinement: 0.962
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No