Information card for entry 4088540

Structure parameters

• Formula: C46 H66 Lu2 N16 Si
• Calculated formula: C47 H42 Lu2 N16 Si
• Title of publication: Tris(pyrazolyl)methanide Complexes of Trivalent Rare-Earth Metals
• Authors of publication: Li, Tengfei; Zhang, Guangchao; Guo, Jingjing; Wang, Shaowu; Leng, Xuebing; Chen, Yaofeng
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 10
• Pages of publication: 1565
• a: 13.8939 ± 0.0013 Å
• b: 17.3468 ± 0.0017 Å
• c: 11.7131 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2823 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 5
• Space group number: 59
• Hermann-Mauguin space group symbol: P m m n :2
• Hall space group symbol: -P 2ab 2a
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.1111
• Weighted residual factors for all reflections included in the refinement: 0.1185
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No