Information card for entry 4088593

Structure parameters

• Formula: C49 H70 Cl2 Ho2 Li N7 O Si2
• Calculated formula: C49 H70 Cl2 Ho2 Li N7 O Si2
• Title of publication: Reactivity of 3-Imino-Functionalized Indoles with Rare-Earth-Metal Amides: Unexpected Substituent Effects on C‒H Activation Pathways and Assembly of Rare-Earth-Metal Complexes
• Authors of publication: Zhu, Xiancui; Li, Yang; Wei, Yun; Wang, Shaowu; Zhou, Shuangliu; Zhang, Lijun
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 11
• Pages of publication: 1838
• a: 15.0287 ± 0.0014 Å
• b: 16.0308 ± 0.0015 Å
• c: 16.6934 ± 0.0015 Å
• α: 84.207 ± 0.001°
• β: 64.952 ± 0.001°
• γ: 78.893 ± 0.001°
• Cell volume: 3574.5 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0451
• Weighted residual factors for significantly intense reflections: 0.0921
• Weighted residual factors for all reflections included in the refinement: 0.099
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No