Crystallography Open Database

Information card for entry 4088602

Preview

Coordinates	4088602.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C186 H330 Er6 N24 Si24
Calculated formula	C186 H330 Er6 N24 Si24
Title of publication	Reactivity of 3-Imino-Functionalized Indoles with Rare-Earth-Metal Amides: Unexpected Substituent Effects on C‒H Activation Pathways and Assembly of Rare-Earth-Metal Complexes
Authors of publication	Zhu, Xiancui; Li, Yang; Wei, Yun; Wang, Shaowu; Zhou, Shuangliu; Zhang, Lijun
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	11
Pages of publication	1838
a	26.9505 ± 0.0008 Å
b	26.9505 ± 0.0008 Å
c	40.167 ± 0.002 Å
α	90°
β	90°
γ	120°
Cell volume	25265.8 ± 1.6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.106
Residual factor for significantly intense reflections	0.0513
Weighted residual factors for significantly intense reflections	0.1248
Weighted residual factors for all reflections included in the refinement	0.1393
Goodness-of-fit parameter for all reflections included in the refinement	0.863
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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