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Information card for entry 4088637
Preview
Coordinates | 4088637.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H53 N Os P2 |
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Calculated formula | C28 H53 N Os P2 |
SMILES | [OsH3]1([P](C(C)C)(C(C)C)C(C)C)([P](C(C)C)(C(C)C)C(C)C)[n]2cc(C)cc3c2c1ccc3 |
Title of publication | Osmium-Mediated Direct C‒H Bond Activation at the 8-Position of Quinolines |
Authors of publication | Esteruelas, Miguel A.; Larramona, Carmen; Oñate, Enrique |
Journal of publication | Organometallics |
Year of publication | 2016 |
Journal volume | 35 |
Journal issue | 11 |
Pages of publication | 1597 |
a | 8.9257 ± 0.0014 Å |
b | 16.717 ± 0.003 Å |
c | 20.972 ± 0.003 Å |
α | 107.975 ± 0.002° |
β | 91.234 ± 0.003° |
γ | 95.736 ± 0.002° |
Cell volume | 2957.1 ± 0.8 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0715 |
Residual factor for significantly intense reflections | 0.0399 |
Weighted residual factors for significantly intense reflections | 0.066 |
Weighted residual factors for all reflections included in the refinement | 0.0745 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.996 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4088637.html
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Users of the data should acknowledge the original authors of the
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