Information card for entry 4088658

Structure parameters

• Formula: C140 H220 B3 Cl8 Li5 N3 Nd3 O17 Si3
• Calculated formula: C138 H156 B3 Cl8 Li5.005 N3 Nd3 O16.5 Si3
• Title of publication: Synthesis and Structure of Silicon-Bridged Boratabenzene Fluorenyl Rare-Earth Metal Complexes
• Authors of publication: Wang, Chunhong; Xiang, Li; Leng, Xuebing; Chen, Yaofeng
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 11
• Pages of publication: 1995
• a: 41.835 ± 0.002 Å
• b: 41.835 ± 0.002 Å
• c: 41.835 ± 0.002 Å
• α: 32.8°
• β: 32.8°
• γ: 32.8°
• Cell volume: 19114.3 ± 1.6 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 9
• Space group number: 167
• Hermann-Mauguin space group symbol: R -3 c :R
• Hall space group symbol: -P 3* 2n
• Residual factor for all reflections: 0.0949
• Residual factor for significantly intense reflections: 0.0732
• Weighted residual factors for significantly intense reflections: 0.2017
• Weighted residual factors for all reflections included in the refinement: 0.2215
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No