Information card for entry 4088691

Structure parameters

• Formula: C39 H46 Au O P
• Calculated formula: C39 H46 Au O P
• Title of publication: Effect of Substitution, Ring Size, and Counterion on the Intermediates Generated in the Gold-Catalyzed Intramolecular Hydroalkoxylation of Allenes
• Authors of publication: Brooner, Rachel E. M.; Brown, Timothy J.; Chee, Mark A.; Widenhoefer, Ross A.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 11
• Pages of publication: 2014
• a: 10.509 ± 0.0006 Å
• b: 12.2859 ± 0.0006 Å
• c: 13.7859 ± 0.0007 Å
• α: 78.988 ± 0.002°
• β: 78.948 ± 0.003°
• γ: 69.197 ± 0.002°
• Cell volume: 1618.31 ± 0.15 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0417
• Residual factor for significantly intense reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.0644
• Weighted residual factors for all reflections included in the refinement: 0.0665
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No