Information card for entry 4088840

Structure parameters

• Formula: C22 H63 Cl2 Ge2 P Si8
• Calculated formula: C22 H63 Cl2 Ge2 P Si8
• Title of publication: Basic Reactivity Pattern of a Cyclic Disilylated Germylene.
• Authors of publication: Walewska, Małgorzata; Hlina, Johann; Baumgartner, Judith; Müller, Thomas; Marschner, Christoph
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 16
• Pages of publication: 2728 - 2737
• a: 11.649 ± 0.002 Å
• b: 19.428 ± 0.004 Å
• c: 19.098 ± 0.004 Å
• α: 90°
• β: 102.65 ± 0.03°
• γ: 90°
• Cell volume: 4217.3 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0797
• Residual factor for significantly intense reflections: 0.067
• Weighted residual factors for significantly intense reflections: 0.1286
• Weighted residual factors for all reflections included in the refinement: 0.133
• Goodness-of-fit parameter for all reflections included in the refinement: 1.267
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No