Information card for entry 4088899

Structure parameters

• Formula: C25 H38 B F4 O2 Rh
• Calculated formula: C25 H38 B F4 O2 Rh
• Title of publication: Cyclobutadiene Arene Complexes of Rhodium and Iridium
• Authors of publication: Shvydkiy, Nikita V.; Trifonova, Evgeniya A.; Shved, Andrei M.; Nelyubina, Yulia V.; Chusov, Denis; Perekalin, Dmitry S.; Kudinov, Alexander R.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 17
• Pages of publication: 3025
• a: 8.817 ± 0.0007 Å
• b: 8.9463 ± 0.0007 Å
• c: 18.1443 ± 0.0014 Å
• α: 95.973 ± 0.002°
• β: 95.706 ± 0.002°
• γ: 110.448 ± 0.002°
• Cell volume: 1319.52 ± 0.18 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0481
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.0856
• Weighted residual factors for all reflections included in the refinement: 0.0914
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No