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Information card for entry 4089069
Preview
Coordinates | 4089069.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C72.5 H89 B F15 N3 Ti |
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Calculated formula | C72.4994 H88.9992 B F15 N3 Ti |
Title of publication | Zwitterionic d0Metal Complexes [(Cy2N)3M]+[(μ-Me)B(C6F5)3]−(M = Ti, Zr, Hf) Derived from Tris(dicyclohexylamido)methyl Metal Precursors |
Authors of publication | Adler, Christian; Frerichs, Nils; Schmidtmann, Marc; Beckhaus, Rüdiger |
Journal of publication | Organometallics |
Year of publication | 2016 |
Journal volume | 35 |
Journal issue | 21 |
Pages of publication | 3728 |
a | 16.927 ± 0.0004 Å |
b | 16.927 ± 0.0004 Å |
c | 39.8167 ± 0.0012 Å |
α | 90° |
β | 90° |
γ | 120° |
Cell volume | 9880 ± 0.4 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 148 |
Hermann-Mauguin space group symbol | R -3 :H |
Hall space group symbol | -R 3 |
Residual factor for all reflections | 0.0722 |
Residual factor for significantly intense reflections | 0.0482 |
Weighted residual factors for significantly intense reflections | 0.1118 |
Weighted residual factors for all reflections included in the refinement | 0.1272 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.002 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4089069.html
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