Information card for entry 4089146

Structure parameters

• Formula: C54 H24 F28 Ge3
• Calculated formula: C54 H24 F28 Ge3
• Title of publication: Oligogermanes Containing Only Electron-Withdrawing Substituents: Synthesis and Properties
• Authors of publication: Zaitsev, Kirill V.; Lam, Kevin; Zhanabil, Zhaisan; Suleimen, Yerlan; Kharcheva, Anastasia V.; Tafeenko, Viktor A.; Oprunenko, Yuri F.; Poleshchuk, Oleg Kh.; Lermontova, Elmira Kh.; Churakov, Andrei V.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 36
• Journal issue: 2
• Pages of publication: 298
• a: 14.6304 ± 0.0003 Å
• b: 23.6872 ± 0.0004 Å
• c: 16.11 ± 0.0004 Å
• α: 90°
• β: 96.599 ± 0.002°
• γ: 90°
• Cell volume: 5546 ± 0.2 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1059
• Residual factor for significantly intense reflections: 0.0711
• Weighted residual factors for significantly intense reflections: 0.1801
• Weighted residual factors for all reflections included in the refinement: 0.1935
• Goodness-of-fit parameter for all reflections included in the refinement: 0.829
• Diffraction radiation wavelength: 1.54186 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No