Information card for entry 4089163

Structure parameters

• Formula: C41.5 H49 Br Cl7 N4 O Os P
• Calculated formula: C41.5 H49 Br Cl7 N4 O Os P
• Title of publication: Osmium(II) Complexes Containing a Dianionic CCCC-Donor Tetradentate Ligand
• Authors of publication: Alabau, Roberto G.; Esteruelas, Miguel A.; Oliván, Montserrat; Oñate, Enrique; Palacios, Adrián U.; Tsai, Jui-Yi; Xia, Chuanjun
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 23
• Pages of publication: 3981
• a: 11.8972 ± 0.0008 Å
• b: 13.1287 ± 0.0008 Å
• c: 16.597 ± 0.0016 Å
• α: 102.145 ± 0.001°
• β: 94.266 ± 0.001°
• γ: 114.786 ± 0.001°
• Cell volume: 2261.9 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0416
• Residual factor for significantly intense reflections: 0.0337
• Weighted residual factors for significantly intense reflections: 0.0839
• Weighted residual factors for all reflections included in the refinement: 0.0882
• Goodness-of-fit parameter for all reflections included in the refinement: 0.88
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No