Information card for entry 4089166

Structure parameters

• Formula: C59.5 H47 Cl3 N4 Os P2
• Calculated formula: C59.5 H47 Cl3 N4 Os P2
• Title of publication: Osmium(II) Complexes Containing a Dianionic CCCC-Donor Tetradentate Ligand
• Authors of publication: Alabau, Roberto G.; Esteruelas, Miguel A.; Oliván, Montserrat; Oñate, Enrique; Palacios, Adrián U.; Tsai, Jui-Yi; Xia, Chuanjun
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 23
• Pages of publication: 3981
• a: 20.47 ± 0.003 Å
• b: 19.715 ± 0.003 Å
• c: 24.976 ± 0.003 Å
• α: 90°
• β: 104.265 ± 0.002°
• γ: 90°
• Cell volume: 9769 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0548
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.1142
• Weighted residual factors for all reflections included in the refinement: 0.1196
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No