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Information card for entry 4089179
Preview
Coordinates | 4089179.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C55 H53 N2 O2 P2 Rh2 |
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Calculated formula | C55 H53 N2 O2 P2 Rh2 |
Title of publication | Synthesis and Reactivity of Phosphine-Quinolinolato Rhodium Complexes: Intermediacy of Vinylidene and (Amino)carbene Complexes in the Catalytic Hydroamination of Terminal Alkynes |
Authors of publication | Takano, Shotaro; Kochi, Takuya; Kakiuchi, Fumitoshi |
Journal of publication | Organometallics |
Year of publication | 2016 |
Journal volume | 35 |
Journal issue | 24 |
Pages of publication | 4112 |
a | 13.3742 ± 0.0006 Å |
b | 23.9873 ± 0.0008 Å |
c | 14.8366 ± 0.0005 Å |
α | 90° |
β | 109.445 ± 0.0012° |
γ | 90° |
Cell volume | 4488.3 ± 0.3 Å3 |
Cell temperature | 93 K |
Ambient diffraction temperature | 93 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0402 |
Residual factor for significantly intense reflections | 0.035 |
Weighted residual factors for significantly intense reflections | 0.0876 |
Weighted residual factors for all reflections included in the refinement | 0.0911 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.069 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4089179.html
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