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Information card for entry 4089213
Preview
Coordinates | 4089213.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H56 N3 O Si3 Y |
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Calculated formula | C22 H56 N3 O Si3 Y |
SMILES | [Y](N(C(C)(C)C)[SiH](C)C)(N(C(C)(C)C)[SiH](C)C)(N([SiH](C)C)C(C)(C)C)[O]1CCCC1 |
Title of publication | β-SiH-Containing Tris(silazido) Rare-Earth Complexes as Homogeneous and Grafted Single-Site Catalyst Precursors for Hydroamination |
Authors of publication | Eedugurala, Naresh; Wang, Zhuoran; Yan, KaKing; Boteju, Kasuni C.; Chaudhary, Umesh; Kobayashi, Takeshi; Ellern, Arkady; Slowing, Igor I.; Pruski, Marek; Sadow, Aaron D. |
Journal of publication | Organometallics |
Year of publication | 2017 |
Journal volume | 36 |
Journal issue | 6 |
Pages of publication | 1142 |
a | 18.9236 ± 0.0015 Å |
b | 15.5196 ± 0.0012 Å |
c | 23.0306 ± 0.0018 Å |
α | 90° |
β | 106.23 ± 0.001° |
γ | 90° |
Cell volume | 6494.2 ± 0.9 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0963 |
Residual factor for significantly intense reflections | 0.0481 |
Weighted residual factors for significantly intense reflections | 0.0925 |
Weighted residual factors for all reflections included in the refinement | 0.11 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4089213.html
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Users of the data should acknowledge the original authors of the
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