Information card for entry 4089216

Structure parameters

• Formula: C32 H60 Ca2 F12 N4 O2 Si4
• Calculated formula: C32 H60 Ca2 F12 N4 O2 Si4
• Title of publication: π Ligands in Alkaline Earth Complexes
• Authors of publication: Roşca, Sorin-Claudiu; Caytan, Elsa; Dorcet, Vincent; Roisnel, Thierry; Carpentier, Jean-François; Sarazin, Yann
• Journal of publication: Organometallics
• Year of publication: 2017
• Journal volume: 36
• Journal issue: 7
• Pages of publication: 1269
• a: 10.3552 ± 0.0014 Å
• b: 11.165 ± 0.002 Å
• c: 11.811 ± 0.002 Å
• α: 95.334 ± 0.009°
• β: 105.458 ± 0.007°
• γ: 114.326 ± 0.007°
• Cell volume: 1166.9 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0717
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for significantly intense reflections: 0.0793
• Weighted residual factors for all reflections included in the refinement: 0.0921
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No