Information card for entry 4089219

Structure parameters

• Formula: C16 H30 Ca F6 N2 O Si2
• Calculated formula: C16 H30 Ca F6 N2 O Si2
• Title of publication: π Ligands in Alkaline Earth Complexes
• Authors of publication: Roşca, Sorin-Claudiu; Caytan, Elsa; Dorcet, Vincent; Roisnel, Thierry; Carpentier, Jean-François; Sarazin, Yann
• Journal of publication: Organometallics
• Year of publication: 2017
• Journal volume: 36
• Journal issue: 7
• Pages of publication: 1269
• a: 9.9272 ± 0.0005 Å
• b: 10.2046 ± 0.0004 Å
• c: 12.6699 ± 0.0006 Å
• α: 87.23 ± 0.002°
• β: 76.121 ± 0.002°
• γ: 67.911 ± 0.002°
• Cell volume: 1153.32 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0645
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.0962
• Weighted residual factors for all reflections included in the refinement: 0.1066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No