Information card for entry 4089277

Structure parameters

• Formula: C24 H49 Bi Br2 Si4
• Calculated formula: C24 H49 Bi Br2 Si4
• SMILES: [Bi](Br)(Br)c1c(cc(cc1C([Si](C)(C)C)[Si](C)(C)C)C(C)(C)C)C([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Inorganic-Salt-Free Reduction in Main-Group Chemistry: Synthesis of a Dibismuthene and a Distibene
• Authors of publication: Majhi, Paresh Kumar; Ikeda, Hideaki; Sasamori, Takahiro; Tsurugi, Hayato; Mashima, Kazushi; Tokitoh, Norihiro
• Journal of publication: Organometallics
• Year of publication: 2017
• Journal volume: 36
• Journal issue: 7
• Pages of publication: 1224
• a: 16.7304 ± 0.0005 Å
• b: 9.4485 ± 0.0002 Å
• c: 22.4685 ± 0.0007 Å
• α: 90°
• β: 107.861 ± 0.001°
• γ: 90°
• Cell volume: 3380.58 ± 0.16 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0712
• Residual factor for significantly intense reflections: 0.0366
• Weighted residual factors for significantly intense reflections: 0.0587
• Weighted residual factors for all reflections included in the refinement: 0.0665
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No