Information card for entry 4089282

Structure parameters

• Formula: C67 H113 Al N2 O3 Si2 Y
• Calculated formula: C67 H113 Al N2 O3 Si2 Y
• Title of publication: Yttrium and Aluminum Alkyl Complexes of a Rigid Bis-Anilido NON-Donor Ligand: Synthesis and Hydroamination Catalysis
• Authors of publication: Motolko, Kelly S. A.; Emslie, David J. H.; Jenkins, Hilary A.
• Journal of publication: Organometallics
• Year of publication: 2017
• Journal volume: 36
• Journal issue: 8
• Pages of publication: 1601
• a: 21.812 ± 0.003 Å
• b: 12.0055 ± 0.0019 Å
• c: 27.328 ± 0.004 Å
• α: 90°
• β: 101.616 ± 0.004°
• γ: 90°
• Cell volume: 7009.7 ± 1.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1998
• Residual factor for significantly intense reflections: 0.1233
• Weighted residual factors for significantly intense reflections: 0.2467
• Weighted residual factors for all reflections included in the refinement: 0.2819
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No