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Information card for entry 4089311
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Coordinates | 4089311.cif |
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Original paper (by DOI) | HTML |
Common name | compound 6iPr2b |
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Formula | C40.5 H62 B Cl N9 O4 Pd |
Calculated formula | C40.5 H53 B Cl N9 O4 Pd |
Title of publication | N/O- and C-Bound (Enolato)palladium Complexes with Hydrotris(pyrazolyl)borato Ligands (TpR: R = iPr2, Me2) Obtained via Dehydrative Condensation between the Hydroxo Complexes TpRPd(Py)OH and Active Methylene Compounds: Factors Determining the Isomer Distribution and Dimerization of Cyano Compounds |
Authors of publication | Kujime, Masato; Hikichi, Shiro; Akita, Munetaka |
Journal of publication | Organometallics |
Year of publication | 2001 |
Journal volume | 20 |
Journal issue | 19 |
Pages of publication | 4049 |
a | 10.378 ± 0.003 Å |
b | 22.092 ± 0.004 Å |
c | 10.381 ± 0.003 Å |
α | 98.428 ± 0.019° |
β | 97.843 ± 0.004° |
γ | 80.516 ± 0.018° |
Cell volume | 2306.7 ± 1 Å3 |
Cell temperature | 213 ± 2 K |
Ambient diffraction temperature | 213 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1316 |
Residual factor for significantly intense reflections | 0.0837 |
Weighted residual factors for significantly intense reflections | 0.2069 |
Weighted residual factors for all reflections included in the refinement | 0.2209 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.231 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4089311.html
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