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Information card for entry 4089319
Preview
Coordinates | 4089319.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C42 H46 I O3 P2 Rh Si |
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Calculated formula | C42 H46 I O3 P2 Rh Si |
SMILES | I[RhH]([P](c1ccccc1)(c1ccccc1)c1ccccc1)([P](c1ccccc1)(c1ccccc1)c1ccccc1)[Si](OCC)(OCC)OCC |
Title of publication | Structure and Properties of Halogeno(hydrido)(triorganosilyl)rhodium(III) Complexes, RhX(H)(SiR1nR23-n)(PPh3)2(X = Cl, I; R1= OSiMe3, OEt, R2= Me). Influence of the Alkoxy Groups and Halo Ligand on Stability and Reactivity of the Complexes |
Authors of publication | Nishihara, Yasushi; Takemura, Miwa; Osakada, Kohtaro |
Journal of publication | Organometallics |
Year of publication | 2002 |
Journal volume | 21 |
Journal issue | 5 |
Pages of publication | 825 |
a | 13.171 ± 0.003 Å |
b | 13.706 ± 0.003 Å |
c | 12.637 ± 0.002 Å |
α | 112.62 ± 0.01° |
β | 101.99 ± 0.02° |
γ | 88.5 ± 0.02° |
Cell volume | 2056.2 ± 0.8 Å3 |
Cell temperature | 296.2 K |
Ambient diffraction temperature | 296.2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0399 |
Residual factor for significantly intense reflections | 0.04 |
Weighted residual factors for all reflections | 0.03 |
Weighted residual factors for all reflections included in the refinement | 0.03 |
Goodness-of-fit parameter for all reflections | 1.652 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.65 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4089319.html
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