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Information card for entry 4089338
Preview
Coordinates | 4089338.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | [RuCp(kappa^2^(P,P)-PPh~2~NHC~6~H~4~PPh~2~)(kappa^1^(N)-NH~2~Ph)] SbF~6~.solv (4.solv) |
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Formula | C41 H37 F6 N2 P2 Ru Sb |
Calculated formula | C44.01 H37 F6 N2 P2 Ru Sb |
Title of publication | Reactions of the Cationic Fragments [RuCp(PPh2NHR)2]+and [RuTp(PPh2NHR)2]+(R = Ph,n-Pr) with Alkynes: Formation of Four-Membered Azaphosphacarbenes |
Authors of publication | Pavlik, Sonja; Mereiter, Kurt; Puchberger, Michael; Kirchner, Karl |
Journal of publication | Organometallics |
Year of publication | 2005 |
Journal volume | 24 |
Journal issue | 14 |
Pages of publication | 3561 |
a | 11.142 ± 0.0019 Å |
b | 15.037 ± 0.003 Å |
c | 24.94 ± 0.004 Å |
α | 90° |
β | 100.654 ± 0.003° |
γ | 90° |
Cell volume | 4106.5 ± 1.3 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0735 |
Residual factor for significantly intense reflections | 0.0468 |
Weighted residual factors for significantly intense reflections | 0.097 |
Weighted residual factors for all reflections included in the refinement | 0.1076 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4089338.html
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