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Information card for entry 4089419
Preview
Coordinates | 4089419.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H34 P2 Pd |
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Calculated formula | C24 H34 P2 Pd |
SMILES | C[P](C)(C)[Pd]1(C/C(=C\c2ccccc2)/C(=C/c2ccccc2)C1)[P](C)(C)C |
Title of publication | Synthesis and Reactivity of Five-Membered Palladalactones from Arylallenes and Carbon Dioxide: Relevance to Catalytic Lactone Synthesis |
Authors of publication | Choi, Jun-Chul; Shiraishi, Kouichi; Takenaka, Yasumasa; Yasuda, Hiroyuki; Sakakura, Toshiyasu |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 11 |
Pages of publication | 3411 |
a | 11.5722 ± 0.0007 Å |
b | 15.5202 ± 0.0009 Å |
c | 13.4168 ± 0.0008 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2409.7 ± 0.2 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 4 |
Space group number | 60 |
Hermann-Mauguin space group symbol | P b c n |
Hall space group symbol | -P 2n 2ab |
Residual factor for all reflections | 0.0311 |
Residual factor for significantly intense reflections | 0.0262 |
Weighted residual factors for significantly intense reflections | 0.0706 |
Weighted residual factors for all reflections included in the refinement | 0.0779 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4089419.html
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