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Information card for entry 4089442
Preview
Coordinates | 4089442.cif |
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Original paper (by DOI) | HTML |
Formula | C20 H27 Cl O6 Si |
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Calculated formula | C20 H27 Cl O6 Si |
SMILES | ClC[Si](c1c(OC)cc(OC)cc1OC)(C)c1c(OC)cc(OC)cc1OC |
Title of publication | Synthesis of Silicon-Functionalized (Silylmethyl)silanes and α,ω-Dichlorocarbosilanes Using the TMOP (2,4,6-Trimethoxyphenyl) Protecting Group: (TMOP)Me2SiCH2Cl and (TMOP)2MeSiCH2Cl as Reagents To Introduce the ClMe2SiCH2, MeOMe2SiCH2, or Cl2MeSiCH2 Group by Nucleophilic Substitution at Silicon |
Authors of publication | Laskowski, Nadine; Reis, Eva-Maria; Kötzner, Lisa; Baus, Johannes A.; Burschka, Christian; Tacke, Reinhold |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 11 |
Pages of publication | 3269 |
a | 11.083 ± 0.002 Å |
b | 12.489 ± 0.003 Å |
c | 17.159 ± 0.004 Å |
α | 71.17 ± 0.03° |
β | 73.89 ± 0.03° |
γ | 78.16 ± 0.03° |
Cell volume | 2142.2 ± 0.9 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0738 |
Residual factor for significantly intense reflections | 0.0575 |
Weighted residual factors for significantly intense reflections | 0.1611 |
Weighted residual factors for all reflections included in the refinement | 0.1694 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.078 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4089442.html
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