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Information card for entry 4089484
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Coordinates | 4089484.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | B6 in manuscript |
---|---|
Formula | C54 H59 B F24 Ni O2 P2 |
Calculated formula | C54 H59 B F24 Ni O2 P2 |
Title of publication | Mechanistic Details of the Nickel-Mediated Formation of Acrylates from CO2, Ethylene and Methyl Iodide |
Authors of publication | Plessow, Philipp N.; Weigel, Laura; Lindner, Ronald; Schäfer, Ansgar; Rominger, Frank; Limbach, Michael; Hofmann, Peter |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 11 |
Pages of publication | 3327 |
a | 18.8623 ± 0.0015 Å |
b | 24.459 ± 0.002 Å |
c | 25.783 ± 0.002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 11895.1 ± 1.6 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 7 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0854 |
Residual factor for significantly intense reflections | 0.0507 |
Weighted residual factors for significantly intense reflections | 0.1148 |
Weighted residual factors for all reflections included in the refinement | 0.1345 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4089484.html
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