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Information card for entry 4089529
Preview
Coordinates | 4089529.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H29 O10 P3 W2 |
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Calculated formula | C22 H29 O10 P3 W2 |
Title of publication | Versatile Reactivity of Bridged Pentelidene Complexes toward Secondary and Tertiary Phosphines |
Authors of publication | Stubenhofer, Markus; Kuntz, Christian; Bodensteiner, Michael; Timoshkin, Alexey Y.; Scheer, Manfred |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 12 |
Pages of publication | 3521 |
a | 21.8086 ± 0.0002 Å |
b | 8.795 ± 0.0001 Å |
c | 16.1926 ± 0.0001 Å |
α | 90° |
β | 104.565 ± 0.001° |
γ | 90° |
Cell volume | 3006.04 ± 0.05 Å3 |
Cell temperature | 123 ± 1 K |
Ambient diffraction temperature | 123 ± 1 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0207 |
Residual factor for significantly intense reflections | 0.0182 |
Weighted residual factors for significantly intense reflections | 0.0439 |
Weighted residual factors for all reflections included in the refinement | 0.0448 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.065 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4089529.html
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structural data.