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Information card for entry 4089555
Preview
Coordinates | 4089555.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C42 H34 Cl N O6 |
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Calculated formula | C42 H34 Cl N O6 |
SMILES | Clc1ccc2N(C(=O)[C@]3(O[C@@H](CC3(C(=O)OC(c3ccccc3)c3ccccc3)C(=O)OC(c3ccccc3)c3ccccc3)C=C)c2c1)C |
Title of publication | Diastereo- and Enantioselective Construction of Oxindole-Fused Spirotetrahydrofuran Scaffolds through Palladium-Catalyzed Asymmetric [3+2] Cycloaddition of Vinyl Cyclopropanes and Isatins |
Authors of publication | Mei, Liang-yong; Wei, Yin; Xu, Qin; Shi, Min |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 12 |
Pages of publication | 3544 |
a | 12.403 ± 0.0013 Å |
b | 15.0871 ± 0.0016 Å |
c | 18.968 ± 0.002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3549.4 ± 0.6 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0665 |
Residual factor for significantly intense reflections | 0.0459 |
Weighted residual factors for significantly intense reflections | 0.0983 |
Weighted residual factors for all reflections included in the refinement | 0.1088 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.931 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4089555.html
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Users of the data should acknowledge the original authors of the
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