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Information card for entry 4089571
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Coordinates | 4089571.cif |
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Original paper (by DOI) | HTML |
Common name | [(dtbpf)PdCl][SbCl6].0.5(CH2Cl2) |
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Formula | C26.5 H45 Cl8 Fe P2 Pd Sb |
Calculated formula | C26.5 H45 Cl8 Fe P2 Pd Sb |
Title of publication | Palladium(II) and Platinum(II) Compounds of 1,1′-Bis(phosphino)metallocene (M = Fe, Ru) Ligands with Metal‒Metal Interactions |
Authors of publication | Gramigna, Kathryn M.; Oria, Jeremy V.; Mandell, Chelsea L.; Tiedemann, Margaret A.; Dougherty, William G.; Piro, Nicholas A.; Kassel, W. Scott; Chan, Benny C.; Diaconescu, Paula L.; Nataro, Chip |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 20 |
Pages of publication | 5966 |
a | 11.495 ± 0.01 Å |
b | 16.945 ± 0.014 Å |
c | 19.559 ± 0.016 Å |
α | 90° |
β | 97.657 ± 0.011° |
γ | 90° |
Cell volume | 3776 ± 5 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1025 |
Residual factor for significantly intense reflections | 0.0687 |
Weighted residual factors for significantly intense reflections | 0.1658 |
Weighted residual factors for all reflections included in the refinement | 0.1797 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.076 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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