Crystallography Open Database

Information card for entry 4089657

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Coordinates	4089657.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H49 Cl N4 O4 Rh
Calculated formula	C33 H49 Cl N4 O4 Rh
Title of publication	Rhodium(I) Complexes of the Conformationally Rigid IBioxMe4 Ligand: Preparation of Mono-, Bis-, and Tris-ligated NHC Complexes
Authors of publication	Chaplin, Adrian B.
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	12
Pages of publication	3069
a	10.60751 ± 0.00016 Å
b	16.42 ± 0.0003 Å
c	20.2981 ± 0.0004 Å
α	70.9975 ± 0.0015°
β	79.908 ± 0.0014°
γ	84.7055 ± 0.0013°
Cell volume	3288.69 ± 0.11 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0419
Residual factor for significantly intense reflections	0.0335
Weighted residual factors for significantly intense reflections	0.0781
Weighted residual factors for all reflections included in the refinement	0.0826
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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