Information card for entry 4089662

Structure parameters

• Formula: C23 H32 Cl N4 O5 Rh
• Calculated formula: C23 H32 Cl N4 O5 Rh
• Title of publication: Rhodium(I) Complexes of the Conformationally Rigid IBioxMe4 Ligand: Preparation of Mono-, Bis-, and Tris-ligated NHC Complexes
• Authors of publication: Chaplin, Adrian B.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 12
• Pages of publication: 3069
• a: 10.23498 ± 0.00017 Å
• b: 11.4086 ± 0.0002 Å
• c: 10.78784 ± 0.00018 Å
• α: 90°
• β: 99.6132 ± 0.0016°
• γ: 90°
• Cell volume: 1241.97 ± 0.04 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0375
• Residual factor for significantly intense reflections: 0.0294
• Weighted residual factors for significantly intense reflections: 0.065
• Weighted residual factors for all reflections included in the refinement: 0.0686
• Goodness-of-fit parameter for all reflections included in the refinement: 1.13
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Duplicate of: 4089661
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No