Information card for entry 4089683

Structure parameters

• Formula: C52 H56 N2 P Ta
• Calculated formula: C52 H56 N2 P Ta
• Title of publication: Carbon‒Carbon Bond Forming Reactions with Tantalum Diamidophosphine Complexes That Incorporate Alkyne Ligands
• Authors of publication: Parker, Kyle D. J.; Fryzuk, Michael D.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 21
• Pages of publication: 6122
• a: 11.1759 ± 0.0004 Å
• b: 33.5707 ± 0.0011 Å
• c: 12.7008 ± 0.0004 Å
• α: 90°
• β: 99.101 ± 0.001°
• γ: 90°
• Cell volume: 4705.1 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173.15 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0419
• Residual factor for significantly intense reflections: 0.0281
• Weighted residual factors for significantly intense reflections: 0.0575
• Weighted residual factors for all reflections included in the refinement: 0.0604
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No