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Information card for entry 4089698
Preview
Coordinates | 4089698.cif |
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Original paper (by DOI) | HTML |
Formula | C49 H111 Cl2 Nd O16 Si4 |
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Calculated formula | C49 H111 Cl2 Nd O16 Si4 |
Title of publication | Synthesis and Characterization of Rare Earth Siloxide Complexes, M[OSi(OtBu)3]3(L)x where L is HOSi(OtBu)3 and x = 0 or 1 |
Authors of publication | Lapadula, Giuseppe; Conley, Matthew P.; Copéret, Christophe; Andersen, Richard A. |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 34 |
Journal issue | 11 |
Pages of publication | 2271 |
a | 13.485 ± 0.003 Å |
b | 22.616 ± 0.004 Å |
c | 24.217 ± 0.005 Å |
α | 71.842 ± 0.003° |
β | 89.146 ± 0.003° |
γ | 80.549 ± 0.003° |
Cell volume | 6917 ± 2 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.109 |
Residual factor for significantly intense reflections | 0.1013 |
Weighted residual factors for significantly intense reflections | 0.2454 |
Weighted residual factors for all reflections included in the refinement | 0.2496 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.203 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4089698.html
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