Information card for entry 4089700

Structure parameters

• Formula: C49 H111 Cl2 O16 Sc Si4
• Calculated formula: C49 H111 Cl2 O16 Sc Si4
• Title of publication: Synthesis and Characterization of Rare Earth Siloxide Complexes, M[OSi(OtBu)3]3(L)x where L is HOSi(OtBu)3 and x = 0 or 1
• Authors of publication: Lapadula, Giuseppe; Conley, Matthew P.; Copéret, Christophe; Andersen, Richard A.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2271
• a: 13.7383 ± 0.0013 Å
• b: 14.4897 ± 0.0014 Å
• c: 17.4579 ± 0.0017 Å
• α: 97.5573 ± 0.0013°
• β: 91.3154 ± 0.0013°
• γ: 99.3144 ± 0.0013°
• Cell volume: 3396.1 ± 0.6 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0439
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for significantly intense reflections: 0.0993
• Weighted residual factors for all reflections included in the refinement: 0.1047
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No