Information card for entry 4089717

Structure parameters

• Common name: [(PhCOCOPh)Sn{(C(SiMe3)2SiMe2CH2)2}]
• Formula: C34 H62 O2 Si6 Sn
• Calculated formula: C34 H62 O2 Si6 Sn
• Title of publication: Reactions of a Highly Crowded Cyclic Stannylene with Iodoalkanes, Enones, and Dienes. Inhibition of Nucleophilic Substitution at Tin(IV) Centers
• Authors of publication: Asadi, Ashrafolmolouk; Eaborn, Colin; Hill, Michael S.; Hitchcock, Peter B.; Meehan, Margaret M.; Smith, J. David
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 12
• Pages of publication: 2430
• a: 14.4034 ± 0.0005 Å
• b: 18.5094 ± 0.0011 Å
• c: 15.9964 ± 0.0007 Å
• α: 90°
• β: 104.854 ± 0.003°
• γ: 90°
• Cell volume: 4122.1 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.069
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.1346
• Weighted residual factors for all reflections included in the refinement: 0.1474
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No