Crystallography Open Database

Information card for entry 4101254

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Coordinates	4101254.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C84 H84 Cl8 Cu4 N4 P4
Calculated formula	C84 H84 Cl8 Cu4 N4 P4
Title of publication	The alpha-iminophospholide ligands.
Authors of publication	Grundy, Joanna; Donnadieu, Bruno; Mathey, François
Journal of publication	Journal of the American Chemical Society
Year of publication	2006
Journal volume	128
Journal issue	24
Pages of publication	7716 - 7717
a	14.9291 ± 0.0003 Å
b	17.6446 ± 0.0004 Å
c	17.8388 ± 0.0004 Å
α	67.097 ± 0.001°
β	79.278 ± 0.001°
γ	67.324 ± 0.001°
Cell volume	3990.42 ± 0.15 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	160 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0335
Residual factor for significantly intense reflections	0.0265
Weighted residual factors for significantly intense reflections	0.0688
Weighted residual factors for all reflections included in the refinement	0.074
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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