Information card for entry 4101357

Structure parameters

• Formula: C90 H154 N12 O38 Ru6
• Calculated formula: C90 H102 N12 O38 Ru6
• Title of publication: Bridged dihydroxypyridine ligands for the synthesis of expanded helicates.
• Authors of publication: Grote, Zacharias; Bonazzi, Simone; Scopelliti, Rosario; Severin, Kay
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2006
• Journal volume: 128
• Journal issue: 32
• Pages of publication: 10382 - 10383
• a: 24.471 ± 0.005 Å
• b: 14.566 ± 0.003 Å
• c: 31.674 ± 0.006 Å
• α: 90°
• β: 91.08 ± 0.03°
• γ: 90°
• Cell volume: 11288 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.1567
• Residual factor for significantly intense reflections: 0.0868
• Weighted residual factors for significantly intense reflections: 0.1933
• Weighted residual factors for all reflections included in the refinement: 0.2397
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No