Information card for entry 4101717

Structure parameters

• Formula: C34 H57 La N4 Si
• Calculated formula: C34.17 H57 La N4 Si0.93
• Title of publication: Organolanthanide-based synthesis of 1,2,3-triazoles from nitriles and diazo compounds.
• Authors of publication: Evans, William J.; Montalvo, Elizabeth; Champagne, Timothy M.; Ziller, Joseph W.; DiPasquale, Antonio G.; Rheingold, Arnold L.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2008
• Journal volume: 130
• Journal issue: 1
• Pages of publication: 16 - 17
• a: 10.6329 ± 0.0009 Å
• b: 18.1349 ± 0.0016 Å
• c: 19.8862 ± 0.0018 Å
• α: 90°
• β: 104.163 ± 0.002°
• γ: 90°
• Cell volume: 3718 ± 0.6 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.034
• Residual factor for significantly intense reflections: 0.0246
• Weighted residual factors for significantly intense reflections: 0.0591
• Weighted residual factors for all reflections included in the refinement: 0.0638
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No