Information card for entry 4101990

Structure parameters

• Formula: C30 H36.67 N2 O4.33 S2
• Calculated formula: C30 H35.3333 N2 O4.33333 S2
• Title of publication: Total Synthesis of (+)-Fendleridine (Aspidoalbidine) and (+)-1-Acetylaspidoalbidine
• Authors of publication: Erica L. Campbell; Andrea M. Zuhl; Christopher M. Liu; Dale L. Boger
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 3009 - 3012
• a: 7.9428 ± 0.0016 Å
• b: 27.42 ± 0.006 Å
• c: 40.909 ± 0.008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8910 ± 3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1836
• Residual factor for significantly intense reflections: 0.099
• Weighted residual factors for significantly intense reflections: 0.2048
• Weighted residual factors for all reflections included in the refinement: 0.251
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No