Information card for entry 4102059

Structure parameters

• Common name: [N(n-Bu)4][(u-N)(U(N[t-Bu][3,5-Me2C6H3])3)2]
• Formula: C96 H164 N8 O2 U2
• Calculated formula: C96 H164 N8 O2 U2
• Title of publication: Uranium-Nitrogen Multiple Bonding: Isostructural Anionic, Neutral, and Cationic Uranium Nitride Complexes Featuring a Linear U=N=U Core
• Authors of publication: Alexander R. Fox; Polly L. Arnold; Christopher C. Cummins
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 3250 - 3251
• a: 19.0179 ± 0.0009 Å
• b: 21.6348 ± 0.001 Å
• c: 23.6014 ± 0.0011 Å
• α: 90°
• β: 94.932 ± 0.001°
• γ: 90°
• Cell volume: 9674.8 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1054
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.074
• Weighted residual factors for all reflections included in the refinement: 0.0921
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No